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(continued)

(e) Final assembly and inspection requirements. Each sampler shall be tested after manufacture and before delivery to the final user. Each manufacturer shall document its post-manufacturing test procedures. As a minimum, each test shall consist of the following: Tests of the overall integrity of the sampler, including leak tests; calibration or verification of the calibration of the flow measurement device, barometric pressure sensor, and temperature sensors; and operation of the sampler with a filter in place over a period of at least 48 hours. The results of each test shall be suitably documented and shall be subject to review by an ISO-certified auditor.

(f) Manufacturer's audit checklists. Manufacturers shall require an ISO-certified auditor to sign and date a statement indicating that the auditor is aware of the appropriate manufacturing specifications contained in 40 CFR part 50, appendix L, and the test or verification requirements in this subpart. Manufacturers shall also require an ISO-certified auditor to complete the checklists, shown in figures E–1 and E–2 of this subpart, which describe the manufacturer's ability to meet the requirements of the standard for both designation testing and product manufacture.

(1) Designation testing checklist. The completed statement and checklist as shown in figure E–1 of this subpart shall be submitted with the application for reference or equivalent method determination.

(2) Product manufacturing checklist. Manufacturers shall require an ISO-certified auditor to complete a Product Manufacturing Checklist (figure E–2 of this subpart), which evaluates the manufacturer on its ability to meet the requirements of the standard in maintaining quality control in the production of reference or equivalent devices. The initial completed checklist shall be submitted with the application for reference or equivalent method determination. Also, this checklist (figure E–2 of this subpart) must be completed and submitted annually to retain a reference or equivalent method designation for a PM2.5 method.

(3) Phase-in period. If the conditions of paragraph (b)(2) of this section apply, a candidate reference or equivalent method for PM2.5 may be conditionally designated as a reference or equivalent method under this part 53 without the submission of the checklists described in paragraphs (f)(1) and (f)(2) of this section. Such conditional designation shall expire 1 year after the date of the Federal Register notice of the conditional designation unless the checklists are submitted at least 30 days prior to the expiration date.

[62 FR 38799, July 18, 1997; 63 FR 7714, Feb. 17, 1998]

§ 53.52 Leak check test.
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(a) Overview. In section 7.4.6 of 40 CFR part 50, appendix L, the sampler is required to include the facility, including components, instruments, operator controls, a written procedure, and other capabilities as necessary, to allow the operator to carry out a leak test of the sampler at a field monitoring site without additional equipment. This test procedure is intended to test the adequacy and effectiveness of the sampler's leak check facility. Because of the variety of potential sampler configurations and leak check procedures possible, some adaptation of this procedure may be necessary to accommodate the specific sampler under test. The test conditions and performance specifications associated with this test are summarized in table E–1 of this subpart. The candidate test sampler must meet all test parameters and test specifications to successfully pass this test.

(b) Technical definitions. (1) External leakage includes the total flow rate of external ambient air which enters the sampler other than through the sampler inlet and which passes through any one or more of the impactor, filter, or flow rate measurement components.

(2) Internal leakage is the total sample air flow rate that passes through the filter holder assembly without passing through the sample filter.

(c) Required test equipment. (1) Flow rate measurement device, range 70 mL/min to 130 mL/min, 2 percent certified accuracy, NIST-traceable.

(2) Flow rate measurement adaptor (40 CFR part 50, appendix L, figure L-30) or equivalent adaptor to facilitate measurement of sampler flow rate at the top of the downtube.

(3) Impermeable membrane or disk, 47 mm nominal diameter.

(4) Means, such as a micro-valve, of providing a simulated leak flow rate through the sampler of approximately 80 mL/min under the conditions specified for the leak check in the sampler's leak check procedure.

(5) Teflon sample filter, as specified in section 6 of 40 CFR part 50, appendix L.

(d) Calibration of test measurement instruments. Submit documentation showing evidence of appropriately recent calibration, certification of calibration accuracy, and NIST-traceability (if required) of all measurement instruments used in the tests. The accuracy of flow rate meters shall be verified at the highest and lowest pressures and temperatures used in the tests and shall be checked at zero and one or more non-zero flow rates within 7 days of use for this test.

(e) Test setup. (1) The test sampler shall be set up for testing as described in the sampler's operation or instruction manual referred to in §53.4(b)(3). The sampler shall be installed upright and set up in its normal configuration for collecting PM2.5 samples, except that the sample air inlet shall be removed and the flow rate measurement adaptor shall be installed on the sampler's downtube.

(2) The flow rate control device shall be set up to provide a constant, controlled flow rate of 80 mL/min into the sampler downtube under the conditions specified for the leak check in the sampler's leak check procedure.

(3) The flow rate measurement device shall be set up to measure the controlled flow rate of 80 mL/min into the sampler downtube under the conditions specified for the leak check in the sampler's leak check procedure.

(f) Procedure. (1) Install the impermeable membrane in a filter cassette and install the cassette into the sampler. Carry out the internal leak check procedure as described in the sampler's operation/instruction manual and verify that the leak check acceptance criterion specified in table E–1 of this subpart is met.

(2) Replace the impermeable membrane with a Teflon filter and install the cassette in the sampler. Remove the inlet from the sampler and install the flow measurement adaptor on the sampler's downtube. Close the valve of the adaptor to seal the flow system. Conduct the external leak check procedure as described in the sampler's operation/instruction manual and verify that the leak check acceptance criteria specified in table E–1 of this subpart are met.

(3) Arrange the flow control device, flow rate measurement device, and other apparatus as necessary to provide a simulated leak flow rate of 80 mL/min into the test sampler through the downtube during the specified external leak check procedure. Carry out the external leak check procedure as described in the sampler's operation/instruction manual but with the simulated leak of 80 mL/min.

(g) Test results. The requirements for successful passage of this test are:

(1) That the leak check procedure indicates no significant external or internal leaks in the test sampler when no simulated leaks are introduced.

(2) That the leak check procedure properly identifies the occurrence of the simulated external leak of 80 mL/min.

§ 53.53 Test for flow rate accuracy, regulation, measurement accuracy, and cut-off.
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(a) Overview. This test procedure is designed to evaluate a candidate sampler's flow rate accuracy with respect to the design flow rate, flow rate regulation, flow rate measurement accuracy, coefficient of variability measurement accuracy, and the flow rate cut-off function. The tests for the first four parameters shall be conducted over a 6-hour time period during which reference flow measurements are made at intervals not to exceed 5 minutes. The flow rate cut-off test, conducted separately, is intended to verify that the sampler carries out the required automatic sample flow rate cut-off function properly in the event of a low-flow condition. The test conditions and performance specifications associated with this test are summarized in table E–1 of this subpart. The candidate test sampler must meet all test parameters and test specifications to successfully pass this test.

(b) Technical definitions. (1) Sample flow rate means the quantitative volumetric flow rate of the air stream caused by the sampler to enter the sampler inlet and pass through the sample filter, measured in actual volume units at the temperature and pressure of the air as it enters the inlet.

(2) The flow rate cut-off function requires the sampler to automatically stop sample flow and terminate the current sample collection if the sample flow rate deviates by more than the variation limits specified in table E–1 of this subpart (±10 percent from the nominal sample flow rate) for more than 60 seconds during a sample collection period. The sampler is also required to properly notify the operator with a flag warning indication of the out-of-specification flow rate condition and if the flow rate cut-off results in an elapsed sample collection time of less than 23 hours.

(c) Required test equipment. (1) Flow rate meter, suitable for measuring and recording the actual volumetric sample flow rate at the sampler downtube, with a minimum range of 10 to 25 L/min, 2 percent certified, NIST-traceable accuracy. Optional capability for continuous (analog) recording capability or digital recording at intervals not to exceed 30 seconds is recommended. While a flow meter which provides a direct indication of volumetric flow rate is preferred for this test, an alternative certified flow measurement device may be used as long as appropriate volumetric flow rate corrections are made based on measurements of actual ambient temperature and pressure conditions.

(2) Ambient air temperature sensor, with a resolution of 0.1 °C and certified to be accurate to within 0.5 °C (if needed). If the certified flow meter does not provide direct volumetric flow rate readings, ambient air temperature measurements must be made using continuous (analog) recording capability or digital recording at intervals not to exceed 5 minutes.

(3) Barometer, range 600 mm Hg to 800 mm Hg, certified accurate to 2 mm Hg (if needed). If the certified flow meter does not provide direct volumetric flow rate readings, ambient pressure measurements must be made using continuous (analog) recording capability or digital recording at intervals not to exceed 5 minutes.

(4) Flow measurement adaptor (40 CFR part 50, appendix L, figure L-30) or equivalent adaptor to facilitate measurement of sample flow rate at the sampler downtube.

(5) Valve or other means to restrict or reduce the sample flow rate to a value at least 10 percent below the design flow rate (16.67 L/min). If appropriate, the valve of the flow measurement adaptor may be used for this purpose.

(6) Means for creating an additional pressure drop of 55 mm Hg in the sampler to simulate a heavily loaded filter, such as an orifice or flow restrictive plate installed in the filter holder or a valve or other flow restrictor temporarily installed in the flow path near the filter.

(7) Teflon sample filter, as specified in section 6 of 40 CFR part 50, appendix L (if required).

(d) Calibration of test measurement instruments. Submit documentation showing evidence of appropriately recent calibration, certification of calibration accuracy, and NIST-traceability (if required) of all measurement instruments used in the tests. The accuracy of flow-rate meters shall be verified at the highest and lowest pressures and temperatures used in the tests and shall be checked at zero and at least one flow rate within ±3 percent of 16.7 L/min within 7 days prior to use for this test. Where an instrument's measurements are to be recorded with an analog recording device, the accuracy of the entire instrument-recorder system shall be calibrated or verified.

(e) Test setup. (1) Setup of the sampler shall be as required in this paragraph (e) and otherwise as described in the sampler's operation or instruction manual referred to in §53.4(b)(3). The sampler shall be installed upright and set up in its normal configuration for collecting PM2.5 samples. A sample filter and (or) the device for creating an additional 55 mm Hg pressure drop shall be installed for the duration of these tests. The sampler's ambient temperature, ambient pressure, and flow rate measurement systems shall all be calibrated per the sampler's operation or instruction manual within 7 days prior to this test.

(2) The inlet of the candidate sampler shall be removed and the flow measurement adaptor installed on the sampler's downtube. A leak check as described in the sampler's operation or instruction manual shall be conducted and must be properly passed before other tests are carried out.

(3) The inlet of the flow measurement adaptor shall be connected to the outlet of the flow rate meter.

(4) For the flow rate cut-off test, the valve or means for reducing sampler flow rate shall be installed between the flow measurement adaptor and the downtube or in another location within the sampler such that the sampler flow rate can be manually restricted during the test.

(f) Procedure. (1) Set up the sampler as specified in paragraph (e) of this section and otherwise prepare the sampler for normal sample collection operation as directed in the sampler's operation or instruction manual. Set the sampler to automatically start a 6-hour sample collection period at a convenient time.

(2) During the 6-hour operational flow rate portion of the test, measure and record the sample flow rate with the flow rate meter at intervals not to exceed 5 minutes. If ambient temperature and pressure corrections are necessary to calculate volumetric flow rate, ambient temperature and pressure shall be measured at the same frequency as that of the certified flow rate measurements. Note and record the actual start and stop times for the 6-hour flow rate test period.

(3) Following completion of the 6-hour flow rate test period, install the flow rate reduction device and change the sampler flow rate recording frequency to intervals of not more than 30 seconds. Reset the sampler to start a new sample collection period. Manually restrict the sampler flow rate such that the sampler flow rate is decreased slowly over several minutes to a flow rate slightly less than the flow rate cut-off value (15.0 L/min). Maintain this flow rate for at least 2.0 minutes or until the sampler stops the sample flow automatically. Manually terminate the sample period, if the sampler has not terminated it automatically.

(g) Test results. At the completion of the test, validate the test conditions and determine the test results as follows:

(1) Mean sample flow rate. (i) From the certified measurements (Qref) of the test sampler flow rate obtained by use of the flow rate meter, tabulate each flow rate measurement in units of L/min. If ambient temperature and pressure corrections are necessary to calculate volumetric flow rate, each measured flow rate shall be corrected using its corresponding temperature and pressure measurement values. Calculate the mean flow rate for the sample period (Qref,ave) as follows:

Equation 1

where:

n equals the number of discrete certified flow rate measurements over the 6-hour test period.


(ii)(A) Calculate the percent difference between this mean flow rate value and the design value of 16.67 L/min, as follows:

Equation 2
(B) To successfully pass the mean flow rate test, the percent difference calculated in Equation 2 of this paragraph (g)(1)(ii) must be within ±5 percent.

(2) Sample flow rate regulation. (i) From the certified measurements of the test sampler flow rate, calculate the sample coefficient of variation (CV) of the discrete measurements as follows:

Equation 3
(ii) To successfully pass the flow rate regulation test, the calculated coefficient of variation for the certified flow rates must not exceed 2 percent.

(3) Flow rate measurement accuracy. (i) Using the mean volumetric flow rate reported by the candidate test sampler at the completion of the 6-hour test period (Qind,ave), determine the accuracy of the reported mean flow rate as:

Equation 4
(ii) To successfully pass the flow rate measurement accuracy test, the percent difference calculated in Equation 4 of this paragraph (g)(3) shall not exceed 2 percent.

(4) Flow rate coefficient of variation measurement accuracy. (i) Using the flow rate coefficient of variation indicated by the candidate test sampler at the completion of the 6-hour test (%CVind), determine the accuracy of this reported coefficient of variation as:

Equation 5
(ii) To successfully pass the flow rate CV measurement accuracy test, the absolute difference in values calculated in Equation 5 of this paragraph (g)(4) must not exceed 0.3 (CV%).

(5) Flow rate cut-off. (i) Inspect the measurements of the sample flow rate during the flow rate cut-off test and determine the time at which the sample flow rate decreased to a value less than the cut-off value specified in table E–1 of this subpart. To pass this test, the sampler must have automatically stopped the sample flow at least 30 seconds but not more than 90 seconds after the time at which the sampler flow rate was determined to have decreased to a value less than the cut-off value.

(ii) At the completion of the flow rate cut-off test, download the archived data from the test sampler and verify that the sampler's required Flow-out-of-spec and Incorrect sample period flag indicators are properly set.

§ 53.54 Test for proper sampler operation following power interruptions.
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(a) Overview. (1) This test procedure is designed to test certain performance parameters of the candidate sampler during a test period in which power interruptions of various duration occur. The performance parameters tested are:

(i) Proper flow rate performance of the sampler.

(ii) Accuracy of the sampler's average flow rate, CV, and sample volume measurements.

(iii) Accuracy of the sampler's reported elapsed sampling time.

(iv) Accuracy of the reported time and duration of power interruptions.

(2) This test shall be conducted during operation of the test sampler over a continuous 6-hour test period during which the sampler's flow rate shall be measured and recorded at intervals not to exceed 5 minutes. The performance parameters tested under this procedure, the corresponding minimum performance specifications, and the applicable test conditions are summarized in table E–1 of this subpart. Each performance parameter tested, as described or determined in the test procedure, must meet or exceed the associated performance specification to successfully pass this test.

(b) Required test equipment. (1) Flow rate meter, suitable for measuring and recording the actual volumetric sample flow rate at the sampler downtube, with a minimum range of 10 to 25 L/min, 2 percent certified, NIST-traceable accuracy. Optional capability for continuous (analog) recording capability or digital recording at intervals not to exceed 5 minutes is recommended. While a flow meter which provides a direct indication of volumetric flow rate is preferred for this test, an alternative certified flow measurement device may be used as long as appropriate volumetric flow rate corrections are made based on measurements of actual ambient temperature and pressure conditions.

(2) Ambient air temperature sensor (if needed for volumetric corrections to flow rate measurements), with a resolution of 0.1 °C, certified accurate to within 0.5 °C, and continuous (analog) recording capability or digital recording at intervals not to exceed 5 minutes.

(3) Barometer (if needed for volumetric corrections to flow rate measurements), range 600 mm Hg to 800 mm Hg, certified accurate to 2 mm Hg, with continuous (analog) recording capability or digital recording at intervals not to exceed 5 minutes.

(4) Flow measurement adaptor (40 CFR part 50, appendix L, figure L-30) or equivalent adaptor to facilitate measurement of sample flow rate at the sampler downtube.

(5) Means for creating an additional pressure drop of 55 mm Hg in the sampler to simulate a heavily loaded filter, such as an orifice or flow restrictive plate installed in the filter holder or a valve or other flow restrictor temporarily installed in the flow path near the filter.

(6) Teflon sample filter, as specified in section 6 of 40 CFR part 50, appendix L (if required).

(7) Time measurement system, accurate to within 10 seconds per day.

(c) Calibration of test measurement instruments. Submit documentation showing evidence of appropriately recent calibration, certification of calibration accuracy, and NIST-traceability (if required) of all measurement instruments used in the tests. The accuracy of flow rate meters shall be verified at the highest and lowest pressures and temperatures used in the tests and shall be checked at zero and at least one flow rate within ±3 percent of 16.7 L/min within 7 days prior to use for this test. Where an instrument's measurements are to be recorded with an analog recording device, the accuracy of the entire instrument-recorder system shall be calibrated or verified.

(d) Test setup. (1) Setup of the sampler shall be performed as required in this paragraph (d) and otherwise as described in the sampler's operation or instruction manual referred to in §53.4(b)(3). The sampler shall be installed upright and set up in its normal configuration for collecting PM2.5 samples. A sample filter and (or) the device for creating an additional 55 mm Hg pressure drop shall be installed for the duration of these tests. The sampler's ambient temperature, ambient pressure, and flow measurement systems shall all be calibrated per the sampler's operating manual within 7 days prior to this test.

(2) The inlet of the candidate sampler shall be removed and the flow measurement adaptor installed on the sample downtube. A leak check as described in the sampler's operation or instruction manual shall be conducted and must be properly passed before other tests are carried out.

(3) The inlet of the flow measurement adaptor shall be connected to the outlet of the flow rate meter.

(e) Procedure. (1) Set up the sampler as specified in paragraph (d) of this section and otherwise prepare the sampler for normal sample collection operation as directed in the sampler's operation or instruction manual. Set the sampler to automatically start a 6-hour sample collection period at a convenient time.

(2) During the entire 6-hour operational flow rate portion of the test, measure and record the sample flow rate with the flow rate meter at intervals not to exceed 5 minutes. If ambient temperature and pressure corrections are necessary to calculate volumetric flow rate, ambient temperature and pressure shall be measured at the same frequency as that of the certified flow rate measurements. Note and record the actual start and stop times for the 6-hour flow rate test period.

(3) During the 6-hour test period, interrupt the AC line electrical power to the sampler 5 times, with durations of 20 seconds, 40 seconds, 2 minutes, 7 minutes, and 20 minutes (respectively), with not less than 10 minutes of normal electrical power supplied between each power interruption. Record the hour and minute and duration of each power interruption.

(4) At the end of the test, terminate the sample period (if not automatically terminated by the sampler) and download all archived instrument data from the test sampler.

(f) Test results. At the completion of the sampling period, validate the test conditions and determine the test results as follows:

(1) Mean sample flow rate. (i) From the certified measurements (Qref) of the test sampler flow rate, tabulate each flow rate measurement in units of L/min. If ambient temperature and pressure corrections are necessary to calculate volumetric flow rate, each measured flow rate shall be corrected using its corresponding temperature and pressure measurement values. Calculate the mean flow rate for the sample period (Qref,ave) as follows:

Equation 6

where:

n equals the number of discrete certified flow rate measurements over the 6-hour test period, excluding flow rate values obtained during periods of power interruption.


(ii)(A) Calculate the percent difference between this mean flow rate value and the design value of 16.67 L/min, as follows:

Equation 7
(B) To successfully pass this test, the percent difference calculated in Equation 7 of this paragraph (f)(1)(ii) must be within ±5 percent.

(2) Sample flow rate regulation. (i) From the certified measurements of the test sampler flow rate, calculate the sample coefficient of variation of the discrete measurements as follows:

Equation 8
(ii) To successfully pass this test, the calculated coefficient of variation for the certified flow rates must not exceed 2 percent.

(3) Flow rate measurement accuracy. (i) Using the mean volumetric flow rate reported by the candidate test sampler at the completion of the 6-hour test (Qind,ave), determine the accuracy of the reported mean flow rate as:

Equation 9
(ii) To successfully pass this test, the percent difference calculated in Equation 9 of this paragraph (f)(3) shall not exceed 2 percent.

(4) Flow rate CV measurement accuracy. (i) Using the flow rate coefficient of variation indicated by the candidate test sampler at the completion of the 6-hour test (%CVind), determine the accuracy of the reported coefficient of variation as:

Equation 10
(ii) To successfully pass this test, the absolute difference in values calculated in Equation 10 of this paragraph (f)(4) must not exceed 0.3 (CV%).

(5) Verify that the sampler properly provided a record and visual display of the correct year, month, day-of-month, hour, and minute with an accuracy of ±2 minutes, of the start of each power interruption of duration greater than 60 seconds.

(6) Calculate the actual elapsed sample time, excluding the periods of electrical power interruption. Verify that the elapsed sample time reported by the sampler is accurate to within ±20 seconds for the 6-hour test run.

(7) Calculate the sample volume as Qref.ave multiplied by the sample time, excluding periods of power interruption. Verify that the sample volume reported by the sampler is within 2 percent of the calculated sample volume to successfully pass this test.

(8) Inspect the downloaded instrument data from the test sampler and verify that all data are consistent with normal operation of the sampler.

[62 FR 38799, July 18, 1997; 63 FR 7714, Feb. 17, 1998]

§ 53.55 Test for effect of variations in power line voltage and ambient temperature.
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(a) Overview. (1) This test procedure is a combined procedure to test various performance parameters under variations in power line voltage and ambient temperature. Tests shall be conducted in a temperature controlled environment over four 6-hour time periods during which reference temperature and flow rate measurements shall be made at intervals not to exceed 5 minutes. Specific parameters to be evaluated at line voltages of 105 and 125 volts and temperatures of -20 °C and =40 °C are as follows:

(i) Sample flow rate.

(ii) Flow rate regulation.

(iii) Flow rate measurement accuracy.

(iv) Coefficient of variability measurement accuracy.

(v) Ambient air temperature measurement accuracy.

(vi) Proper operation of the sampler when exposed to power line voltage and ambient temperature extremes.

(2) The performance parameters tested under this procedure, the corresponding minimum performance specifications, and the applicable test conditions are summarized in table E–1 of this subpart. Each performance parameter tested, as described or determined in the test procedure, must meet or exceed the associated performance specification given. The candidate sampler must meet all specifications for the associated PM2.5 method to pass this test procedure.

(b) Technical definition. Sample flow rate means the quantitative volumetric flow rate of the air stream caused by the sampler to enter the sampler inlet and pass through the sample filter, measured in actual volume units at the temperature and pressure of the air as it enters the inlet.

(c) Required test equipment. (1) Environmental chamber or other temperature-controlled environment or environments, capable of obtaining and maintaining temperatures at -20 °C and =40 °C as required for the test with an accuracy of ±2 °C. The test environment(s) must be capable of maintaining these temperatures within the specified limits continuously with the additional heat load of the operating test sampler in the environment. Henceforth, where the test procedures specify a test or environmental “chamber,” an alternative temperature-controlled environmental area or areas may be substituted, provided the required test temperatures and all other test requirements are met.

(2) Variable voltage AC power transformer, range 100 Vac to 130 Vac, with sufficient current capacity to operate the test sampler continuously under the test conditions.

(3) Flow rate meter, suitable for measuring and recording the actual volumetric sample flow rate at the sampler downtube, with a minimum range of 10 to 25 actual L/min, 2 percent certified, NIST-traceable accuracy. Optional capability for continuous (analog) recording capability or digital recording at intervals not to exceed 5 minutes is recommended. While a flow meter which provides a direct indication of volumetric flow rate is preferred for this test, an alternative certified flow measurement device may be used as long as appropriate volumetric flow rate corrections are made based on measurements of actual ambient temperature and pressure conditions.

(4) Ambient air temperature recorder, range -30 °C to =50 °C, with a resolution of 0.1 °C and certified accurate to within 0.5 °C. Ambient air temperature measurements must be made using continuous (analog) recording capability or digital recording at intervals not to exceed 5 minutes.

(5) Barometer, range 600 mm Hg to 800 mm Hg, certified accurate to 2 mm Hg. If the certified flow rate meter does not provide direct volumetric flow rate readings, ambient pressure measurements must be made using continuous (analog) recording capability or digital recording at intervals not to exceed 5 minutes.

(6) Flow measurement adaptor (40 CFR part 50, appendix L, figure L-30) or equivalent adaptor to facilitate measurement of sampler flow rate at the sampler downtube.

(7) Means for creating an additional pressure drop of 55 mm Hg in the sampler to simulate a heavily loaded filter, such as an orifice or flow restrictive plate installed in the filter holder or a valve or other flow restrictor temporarily installed in the flow path near the filter.

(8) AC RMS voltmeter, accurate to 1.0 volt.

(9) Teflon sample filter, as specified in section 6 of 40 CFR part 50, appendix L (if required).

(d) Calibration of test measurement instruments. Submit documentation showing evidence of appropriately recent calibration, certification of calibration accuracy, and NIST-traceability (if required) of all measurement instruments used in the tests. The accuracy of flow rate meters shall be verified at the highest and lowest pressures and temperatures used in the tests and shall be checked at zero and at least one flow rate within ±3 percent of 16.7 L/min within 7 days prior to use for this test. Where an instrument's measurements are to be recorded with an analog recording device, the accuracy of the entire instrument-recorder system shall be calibrated or verified.

(e) Test setup. (1) Setup of the sampler shall be performed as required in this paragraph (e) and otherwise as described in the sampler's operation or instruction manual referred to in §53.4(b)(3). The sampler shall be installed upright and set up in the temperature-controlled chamber in its normal configuration for collecting PM2.5 samples. A sample filter and (or) the device for creating an additional 55 mm Hg pressure drop shall be installed for the duration of these tests. The sampler's ambient temperature, ambient pressure, and flow measurement systems shall all be calibrated per the sampler's operating manual within 7 days prior to this test.

(2) The inlet of the candidate sampler shall be removed and the flow measurement adaptor installed on the sampler's downtube. A leak check as described in the sampler's operation or instruction manual shall be conducted and must be properly passed before other tests are carried out.

(3) The inlet of the flow measurement adaptor shall be connected to the outlet of the flow rate meter.

(4) The ambient air temperature recorder shall be installed in the test chamber such that it will accurately measure the temperature of the air in the vicinity of the candidate sampler without being unduly affected by the chamber's air temperature control system.

(f) Procedure. (1) Set up the sampler as specified in paragraph (e) of this section and otherwise prepare the sampler for normal sample collection operation as directed in the sampler's operation or instruction manual.

(2) The test shall consist of four test runs, one at each of the following conditions of chamber temperature and electrical power line voltage (respectively):

(i) -20 °C ±2 °C and 105 ±1 Vac.

(ii) -20 °C ±2 °C and 125 ±1 Vac.

(iii) =40 °C ±2 °C and 105 ±1 Vac.

(iv) =40 °C ±2 °C and 125 ±1 Vac.

(3) For each of the four test runs, set the selected chamber temperature and power line voltage for the test run. Upon achieving each temperature setpoint in the chamber, the candidate sampler and flow meter shall be thermally equilibrated for a period of at least 2 hours prior to the test run. Following the thermal conditioning time, set the sampler to automatically start a 6-hour sample collection period at a convenient time.

(4) During each 6-hour test period:

(i) Measure and record the sample flow rate with the flow rate meter at intervals not to exceed 5 minutes. If ambient temperature and pressure corrections are necessary to calculate volumetric flow rate, ambient temperature and pressure shall be measured at the same frequency as that of the certified flow rate measurements. Note and record the actual start and stop times for the 6-hour flow rate test period.

(ii) Determine and record the ambient (chamber) temperature indicated by the sampler and the corresponding ambient (chamber) temperature measured by the ambient temperature recorder specified in paragraph (c)(4) of this section at intervals not to exceed 5 minutes.

(iii) Measure the power line voltage to the sampler at intervals not greater than 1 hour.

(5) At the end of each test run, terminate the sample period (if not automatically terminated by the sampler) and download all archived instrument data from the test sampler.

(g) Test results. For each of the four test runs, examine the chamber temperature measurements and the power line voltage measurements. Verify that the temperature and line voltage met the requirements specified in paragraph (f) of this section at all times during the test run. If not, the test run is not valid and must be repeated. Determine the test results as follows:

(1) Mean sample flow rate. (i) From the certified measurements (Qref) of the test sampler flow rate, tabulate each flow rate measurement in units of L/min. If ambient temperature and pressure corrections are necessary to calculate volumetric flow rate, each measured flow rate shall be corrected using its corresponding temperature and pressure measurement values. Calculate the mean flow rate for each sample period (Qref,ave) as follows:

Equation 11

where:

n equals the number of discrete certified flow rate measurements over each 6-hour test period.


(ii)(A) Calculate the percent difference between this mean flow rate value and the design value of 16.67 L/min, as follows:

Equation 12
(B) To successfully pass this test, the percent difference calculated in Equation 12 of this paragraph (g)(1)(ii) must be within ±5 percent for each test run.

(2) Sample flow rate regulation. (i) From the certified measurements of the test sampler flow rate, calculate the sample coefficient of variation of the discrete measurements as follows:

Equation 13
(ii) To successfully pass this test, the calculated coefficient of variation for the certified flow rates must not exceed 2 percent.

(3) Flow rate measurement accuracy. (i) Using the mean volumetric flow rate reported by the candidate test sampler at the completion of each 6-hour test (Qind,ave), determine the accuracy of the reported mean flow rate as:

Equation 14
(ii) To successfully pass this test, the percent difference calculated in Equation 14 of this paragraph (g)(3) shall not exceed 2 percent for each test run.

(4) Flow rate coefficient of variation measurement accuracy. (i) Using the flow rate coefficient of variation indicated by the candidate test sampler (%CVind), determine the accuracy of the reported coefficient of variation as:

Equation 15
(ii) To successfully pass this test, the absolute difference calculated in Equation 15 of this paragraph (g)(4) must not exceed 0.3 (CV%) for each test run.

(5) Ambient temperature measurement accuracy. (i) Calculate the absolute value of the difference between the mean ambient air temperature indicated by the test sampler and the mean ambient (chamber) air temperature measured with the ambient air temperature recorder as:

Equation 16

where:

Tind,ave = mean ambient air temperature indicated by the test sampler, °C; and

ref,ave = mean ambient air temperature measured by the reference temperature instrument, °C.


(ii) The calculated temperature difference must be less than 2 °C for each test run.

(6) Sampler functionality. To pass the sampler functionality test, the following two conditions must both be met for each test run:

(i) The sampler must not shutdown during any portion of the 6-hour test.

(ii) An inspection of the downloaded data from the test sampler verifies that all the data are consistent with normal operation of the sampler.

§ 53.56 Test for effect of variations in ambient pressure.
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(a) Overview. (1) This test procedure is designed to test various sampler performance parameters under variations in ambient (barometric) pressure. Tests shall be conducted in a pressure-controlled environment over two 6-hour time periods during which reference pressure and flow rate measurements shall be made at intervals not to exceed 5 minutes. Specific parameters to be evaluated at operating pressures of 600 and 800 mm Hg are as follows:

(i) Sample flow rate.

(ii) Flow rate regulation.

(iii) Flow rate measurement accuracy.

(iv) Coefficient of variability measurement accuracy.

(v) Ambient pressure measurement accuracy.

(vi) Proper operation of the sampler when exposed to ambient pressure extremes.

(2) The performance parameters tested under this procedure, the corresponding minimum performance specifications, and the applicable test conditions are summarized in table E–1 of this subpart. Each performance parameter tested, as described or determined in the test procedure, must meet or exceed the associated performance specification given. The candidate sampler must meet all specifications for the associated PM2.5 method to pass this test procedure.

(b) Technical definition. Sample flow rate means the quantitative volumetric flow rate of the air stream caused by the sampler to enter the sampler inlet and pass through the sample filter, measured in actual volume units at the temperature and pressure of the air as it enters the inlet.

(c) Required test equipment. (1) Hypobaric chamber or other pressure-controlled environment or environments, capable of obtaining and maintaining pressures at 600 mm Hg and 800 mm Hg required for the test with an accuracy of 5 mm Hg. Henceforth, where the test procedures specify a test or environmental chamber, an alternative pressure-controlled environmental area or areas may be substituted, provided the test pressure requirements are met. Means for simulating ambient pressure using a closed-loop sample air system may also be approved for this test; such a proposed method for simulating the test pressure conditions may be described and submitted to EPA at the address given in §53.4(a) prior to conducting the test for a specific individual determination of acceptability.

(2) Flow rate meter, suitable for measuring and recording the actual volumetric sampler flow rate at the sampler downtube, with a minimum range of 10 to 25 L/min, 2 percent certified, NIST-traceable accuracy. Optional capability for continuous (analog) recording capability or digital recording at intervals not to exceed 5 minutes is recommended. While a flow meter which provides a direct indication of volumetric flow rate is preferred for this test, an alternative certified flow measurement device may be used as long as appropriate volumetric flow rate corrections are made based on measurements of actual ambient temperature and pressure conditions.

(3) Ambient air temperature recorder (if needed for volumetric corrections to flow rate measurements) with a range -30 °C to =50 °C, certified accurate to within 0.5 °C. If the certified flow meter does not provide direct volumetric flow rate readings, ambient temperature measurements must be made using continuous (analog) recording capability or digital recording at intervals not to exceed 5 minutes.

(4) Barometer, range 600 mm Hg to 800 mm Hg, certified accurate to 2 mm Hg. Ambient air pressure measurements must be made using continuous (analog) recording capability or digital recording at intervals not to exceed 5 minutes.

(5) Flow measurement adaptor (40 CFR part 50, appendix L, figure L–30) or equivalent adaptor to facilitate measurement of sampler flow rate at the sampler downtube.

(6) Means for creating an additional pressure drop of 55 mm Hg in the sampler to simulate a heavily loaded filter, such as an orifice or flow restrictive plate installed in the filter holder or a valve or other flow restrictor temporarily installed in the flow path near the filter.

(7) Teflon sample filter, as specified in section 6 of 40 CFR part 50, appendix L (if required).

(d) Calibration of test measurement instruments. Submit documentation showing evidence of appropriately recent calibration, certification of calibration accuracy, and NIST-traceability (if required) of all measurement instruments used in the tests. The accuracy of flow rate meters shall be verified at the highest and lowest pressures and temperatures used in the tests and shall be checked at zero and at least one flow rate within ±3 percent of 16.7 L/min within 7 days prior to use for this test. Where an instrument's measurements are to be recorded with an analog recording device, the accuracy of the entire instrument-recorder system shall be calibrated or verified.

(e) Test setup. (1) Setup of the sampler shall be performed as required in this paragraph (e) and otherwise as described in the sampler's operation or instruction manual referred to in §53.4(b)(3). The sampler shall be installed upright and set up in the pressure-controlled chamber in its normal configuration for collecting PM2.5 samples. A sample filter and (or) the device for creating an additional 55 mm Hg pressure drop shall be installed for the duration of these tests. The sampler's ambient temperature, ambient pressure, and flow measurement systems shall all be calibrated per the sampler's operating manual within 7 days prior to this test.

(2) The inlet of the candidate sampler shall be removed and the flow measurement adaptor installed on the sampler's downtube. A leak check as described in the sampler's operation or instruction manual shall be conducted and must be properly passed before other tests are carried out.

(3) The inlet of the flow measurement adaptor shall be connected to the outlet of the flow rate meter.

(4) The barometer shall be installed in the test chamber such that it will accurately measure the air pressure to which the candidate sampler is subjected.

(f) Procedure. (1) Set up the sampler as specified in paragraph (e) of this section and otherwise prepare the sampler for normal sample collection operation as directed in the sampler's operation or instruction manual.

(2) The test shall consist of two test runs, one at each of the following conditions of chamber pressure:

(i) 600 mm Hg.

(ii) 800 mm Hg.

(3) For each of the two test runs, set the selected chamber pressure for the test run. Upon achieving each pressure setpoint in the chamber, the candidate sampler shall be pressure-equilibrated for a period of at least 30 minutes prior to the test run. Following the conditioning time, set the sampler to automatically start a 6-hour sample collection period at a convenient time.

(4) During each 6-hour test period:

(i) Measure and record the sample flow rate with the flow rate meter at intervals not to exceed 5 minutes. If ambient temperature and pressure corrections are necessary to calculate volumetric flow rate, ambient temperature and pressure shall be measured at the same frequency as that of the certified flow rate measurements. Note and record the actual start and stop times for the 6-hour flow rate test period.

(ii) Determine and record the ambient (chamber) pressure indicated by the sampler and the corresponding ambient (chamber) pressure measured by the barometer specified in paragraph (c)(4) of this section at intervals not to exceed 5 minutes.

(5) At the end of each test period, terminate the sample period (if not automatically terminated by the sampler) and download all archived instrument data for the test run from the test sampler.

(g) Test results. For each of the two test runs, examine the chamber pressure measurements. Verify that the pressure met the requirements specified in paragraph (f) of this section at all times during the test. If not, the test run is not valid and must be repeated. Determine the test results as follows:

(1) Mean sample flow rate. (i) From the certified measurements (Qref) of the test sampler flow rate, tabulate each flow rate measurement in units of L/min. If ambient temperature and pressure corrections are necessary to calculate volumetric flow rate, each measured flow rate shall be corrected using its corresponding temperature and pressure measurement values. Calculate the mean flow rate for the sample period (Qref,ave) as follows:

Equation 17

where:

n equals the number of discrete certified flow measurements over the 6-hour test period.


(ii)(A) Calculate the percent difference between this mean flow rate value and the design value of 16.67 L/min, as follows:

Equation 18
(B) To successfully pass this test, the percent difference calculated in Equation 18 of this paragraph (g)(1) must be within ±5 percent for each test run.

(2) Sample flow rate regulation. (i) From the certified measurements of the test sampler flow rate, calculate the sample coefficient of variation of the discrete measurements as follows:

Equation 19
(ii) To successfully pass this test, the calculated coefficient of variation for the certified flow rates must not exceed 2 percent.

(3) Flow rate measurement accuracy. (i) Using the mean volumetric flow rate reported by the candidate test sampler at the completion of each 6-hour test (Qind,ave), determine the accuracy of the reported mean flow rate as:

Equation 20
(ii) To successfully pass this test, the percent difference calculated in Equation 20 of this paragraph (g)(3) shall not exceed 2 percent for each test run.

(4) Flow rate CV measurement accuracy. (i) Using the flow rate coefficient of variation indicated by the candidate test sampler at the completion of the 6-hour test (%CVind), determine the accuracy of the reported coefficient of variation as:

Equation 21
(ii) To successfully pass this test, the absolute difference in values calculated in Equation 21 of this paragraph (g)(4) must not exceed 0.3 (CV%) for each test run.

(5) Ambient pressure measurement accuracy. (i) Calculate the absolute difference between the mean ambient air pressure indicated by the test sampler and the ambient (chamber) air pressure measured with the reference barometer as:

Equation 22

where:

Pind,ave = mean ambient pressure indicated by the test sampler, mm Hg; and

Pref,ave = mean barometric pressure measured by the reference barometer, mm Hg.


(ii) The calculated pressure difference must be less than 10 mm Hg for each test run to pass the test.

(6) Sampler functionality. To pass the sampler functionality test, the following two conditions must both be met for each test run:

(i) The sampler must not shut down during any part of the 6-hour tests; and

(ii) An inspection of the downloaded data from the test sampler verifies that all the data are consistent with normal operation of the sampler.

[62 FR 38799, July 18, 1997; 63 FR 7714, Feb. 17, 1998]

§ 53.57 Test for filter temperature control during sampling and post-sampling periods.
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(a) Overview. This test is intended to measure the candidate sampler's ability to prevent excessive overheating of the PM2.5 sample collection filter (or filters) under conditions of elevated solar insolation. The test evaluates radiative effects on filter temperature during a 4-hour period of active sampling as well as during a subsequent 4-hour non-sampling time period prior to filter retrieval. Tests shall be conducted in an environmental chamber which provides the proper radiant wavelengths and energies to adequately simulate the sun's radiant effects under clear conditions at sea level. For additional guidance on conducting solar radiative tests under controlled conditions, consult military standard specification 810-E (reference 6 in appendix A of this subpart). The performance parameters tested under this procedure, the corresponding minimum performance specifications, and the applicable test conditions are summarized in table E–1 of this subpart. Each performance parameter tested, as described or determined in the test procedure, must meet or exceed the associated performance specification to successfully pass this test. (continued)